2-苯基-1,5-苯并硫氮杂卓-4(5H)-酮合成路线 (共 8 条)
反应条件
in dichloromethane 24 h; Ambient temperature;
参考文献
Hofmann, Hans; Fischer, Herbert; Bremer, Matthias
Chemische Berichte, 1987 , vol. 120, p. 2087 - 2089
反应条件
1: 88 percent / NaH / dimethylsulfoxide / Ambient temperature 2: 36 percent / acetic acid / 24 h / 150 °C View Scheme
参考文献
Kaupp, Gerd; Gruendken, Eleonore; Matthies, Doris
Chemische Berichte, 1986 , vol. 119, # 10 p. 3109 - 3120
反应条件
1: 88 percent / NaH / dimethylsulfoxide / Ambient temperature 2: 4 percent / hydroquinone / benzene / 24 h / 190 °C 3: 12 percent / hydroquinone / benzene / 24 h / 220 °C View Scheme
参考文献
Chemische Berichte, , vol. 119, # 10 p. 3109 - 3120
参考文献
Hofmann, Hans; Fischer, Herbert; Bremer, Matthias
Chemische Berichte, 1987 , vol. 120, p. 2087 - 2089
参考文献
Kaupp, Gerd; Gruendken, Eleonore; Matthies, Doris
Chemische Berichte, 1986 , vol. 119, # 10 p. 3109 - 3120
反应条件
1: Py
2: (i) NaH, dioxane, (ii) ClCH2CH2NMe2
View Scheme
参考文献
Kugita,H. et al.
Chemical and Pharmaceutical Bulletin, 1971 , vol. 19, p. 595 - 602
反应条件
(i) NaH, dioxane, (ii) ClCH2CH2NMe2; Multistep reaction;
参考文献
Kugita,H. et al.
Chemical and Pharmaceutical Bulletin, 1971 , vol. 19, p. 595 - 602
反应条件
1: 88 percent / NaH / dimethylsulfoxide / Ambient temperature
2: 24 percent / hydroquinone / benzene / 24 h / 190 °C
View Scheme
参考文献
Kaupp, Gerd; Gruendken, Eleonore; Matthies, Doris
Chemische Berichte, 1986 , vol. 119, # 10 p. 3109 - 3120