6,7-二氢-5H-喹啉-8-酮合成路线 (共 12 条)
参考文献
Boggs, Sharon; Elitzin, Vassil I.; Gudmundsson, Kristjan; Martin, Michael T.; Sharp, Matthew J.
Organic Process Research and Development, 2009 , vol. 13, # 4 p. 781 - 785
反应条件
manganese(IV) oxide in dichloromethane 18 h;
参考文献
Bridger, Gary; Skerlj, Renato; Kaller, Ai; Harwig, Curtis; Bogucki, David; Wilson, Trevor R.; Crawford, Jason; McEachern, Ernest J.; Atsma, Bem; Nan, Siqiao; Zhou, Yuanxi; Schols, Dominique; Smith, Christopher Dennis; Di Fluri, Maria Rosaria
Patent: US2003/220341 A1, 2003 ;
Location in patent: Page/Page column 9 ;
US 20030220341 A1
反应条件
1: With acetic anhydride; benzaldehyde 17 h; Heating; 2: With ozone in methanol T=-40°C; 0.75 h; Further stages.;
参考文献
Kelly, T. Ross; Lebedev, Rimma L.
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2197 - 2205
反应条件
dimethyl sulfoxide; triethylamine in isopropanol acetate
反应条件
hydrogenchloride in acetone 16 h; Heating;
参考文献
McEachern; Yang; Chen; Skerlj; Bridger
Synthetic Communications, 2003 , vol. 33, # 20 p. 3497 - 3502
参考文献
McEachern, Ernest J.; Bridger, Gary J.; Skupinska, Krystyna A.; Skerlj, Renato T.
Patent: US2003/114679 A1, 2003 ;
反应条件
Sodium tetrachloroaurate(III) in ethanol T=75°C; 16 h;
参考文献
Catalano, John G.; Gudmundsson, Kristjan S.; Svolto, Angilique; Boggs, Sharon D.; Miller, John F.; Spaltenstein, Andrew; Thomson, Michael; Wheelan, Pat; Minick, Doug J.; Phelps, Dean P.; Jenkinson, Stephen
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 7 p. 2186 - 2190
反应条件
palladium on activated charcoal in toluene 24 h; Heating;
参考文献
Molina; Molina, Pedro; Pastor; Pastor, Aurelia; Vilaplana; Vilaplana, Maria Jesus; Foces-Foces; Foces-Foces, Concepcion
Tetrahedron, 1995 , vol. 51, # 4 p. 1265 - 1276
反应条件
1: cyclohexane; CF3SO3H; SbF5 / 1.5 h / 20 °C 2: H2O View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 36, # 3 p. 446 - 447
反应条件
ammonium acetate; sodium cyanoborohydride in ethanol T=130°C; 0.0333333 h; Microwave irradiation;
参考文献
Dong, Li; Aleem, Saadat; Fink, Cynthia A.
Tetrahedron Letters, 2010 , vol. 51, # 39 p. 5210 - 5212