N-亚硝基-N-(乙酰氧基甲基)丁胺合成路线 （共 9 条）
反应条件
1: NaHSO3 / H2O / 0.02 h / 0 °C
2: pyridine / 0.5 h / Ambient temperature
View Scheme
参考文献
Mochizuki, Masataka; Anjo, Takako; Okada, Masashi
Tetrahedron Letters, 1980 , vol. 21, p. 3693 - 3696
反应条件
1: 25 percent / 1 M NOCl / CH2Cl2 / 1.) 1 h, -30 deg C, 2.) 2 h, 0 deg C
2: CH2Cl2 / 12 h / Ambient temperature
View Scheme
参考文献
Mueller, Eduard; Kettler, Regina; Wiessler, Manfred
Liebigs Annalen der Chemie, 1984 , # 8 p. 1468 - 1493
反应条件
in pyridine
0.5 h; Ambient temperature; Yield given;
参考文献
Mochizuki, Masataka; Anjo, Takako; Okada, Masashi
Tetrahedron Letters, 1980 , vol. 21, p. 3693 - 3696
反应条件
in dichloromethane
12 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Mueller, Eduard; Kettler, Regina; Wiessler, Manfred
Liebigs Annalen der Chemie, 1984 , # 8 p. 1468 - 1493
参考文献
Mochizuki; Anjo; Okada
Chemical and Pharmaceutical Bulletin, 1978 , vol. 26, # 12 p. 3905 - 3908
反应条件
dihydrogen peroxide in acetic acid
T=50°C; 2 h;
参考文献
Mochizuki, Masataka; Anjo, Takako; Wakabayashi, Yuko; Sone, Toshie; Okada, Masashi
Tetrahedron Letters, 1980 , vol. 21, p. 1761 - 1764
反应条件
dihydrogen peroxide in methanol
T=25°C;
参考文献
Mochizuki, Masataka; Anjo, Takako; Wakabayashi, Yuko; Sone, Toshie; Okada, Masashi
Tetrahedron Letters, 1980 , vol. 21, p. 1761 - 1764
反应条件
dihydrogen peroxide in methanol
T=25°C;
参考文献
Mochizuki, Masataka; Anjo, Takako; Wakabayashi, Yuko; Sone, Toshie; Okada, Masashi
Tetrahedron Letters, 1980 , vol. 21, p. 1761 - 1764
参考文献
Mochizuki, Masataka; Anjo, Takako; Wakabayashi, Yuko; Sone, Toshie; Okada, Masashi
Tetrahedron Letters, 1980 , vol. 21, p. 1761 - 1764
