potassium methanolate in methanol T=40 - 45°C; electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 0.58 F mol-1; cell voltage 60-110 V;
tri-n-butyl-tin hydride; dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine; 2,2'-azo-bisisobutyronitrile multistep reaction: 80 deg C, benzene; reactions of aliphatic and alicyclic esters of N-hydroxypyridine-2-thione in various solvents at various temperatures; Product distributionMechanism;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
