in neat (no solvent) byproducts: CH3COOH; stoich. mixt. stirred at 180°C (thermotstated oil reactor) for 3 h; CH3COOH stripped by N2 stream, collected in condensor;
参考文献
Di Serio; Tesser; Dimiccoli; Cammarota; Nastasi; Santacesaria
Journal of Molecular Catalysis A: Chemical, 2005 , vol. 239, # 1-2 p. 111 - 115
in chloroform; water Langmuir-Blodgett film prepared; CoCl2*H2O dissolved in water; stearic acid dissolved in chloroform; LB films deposited at monolayer pressure of30 mN/m at 19°C with 3 mm/min dipping speed;
KOH in ethanol; water pptn.; washing (water, ethanol), drying (vac. desiccator, several days), recrystallization (n-hexanol); elem. anal., TG, DSC;
参考文献
Marques, Eduardo F.; Burrows, Hugh D.; Miguel, Maria Da Graca
Journal of the Chemical Society - Faraday Transactions, 1998 , vol. 94, # 12 p. 1729 - 1736
