(3,4-二甲氧基苯基)乙醛合成路线 (共 41 条)
反应条件
2: acetic acid anhydride 3: aq.-ethanolic KOH-solution View Scheme
参考文献
Hahn; Schales
Chemische Berichte, 1934 , vol. 67, p. 1486,1490
Chemische Berichte, 1935 , vol. 68, p. 24,27
反应条件
2: acetic acid anhydride View Scheme
参考文献
Hahn; Schales
Chemische Berichte, 1934 , vol. 67, p. 1486,1490
Chemische Berichte, 1935 , vol. 68, p. 24,27
反应条件
ethanol; nickel Hydrogenation;
参考文献
Kiruthika, Selvarangam E.; Perumal, Paramasivan Thirumalai
Organic Letters, 2014 , vol. 16, # 2 p. 484 - 487
反应条件
und Erwaermen des Reaktionsprodukts mit wss.Salzsaeure;
参考文献
Spaeth; Berger
Chemische Berichte, 1930 , vol. 63, p. 2098,2100
反应条件
2: sodium; ethanol View Scheme
参考文献
Ciencia, , vol. 7, p. 136
反应条件
1: 37 percent / TMSOTf / CCl4; CHCl3 / 24 h / Ambient temperature 2: 82 percent / HCOOH / 5 h / Ambient temperature 3: 86 percent / BH3*THF / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Johnson, A. Peter; Luke, Richard W. A.; Singh, Gurmaj; Boa, Andrew N.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 9 p. 907 - 913
反应条件
hydrogenchloride in 1,4-dioxane
1 h;
参考文献
Maurin, Cedric; Bailly, Fabrice; Cotelle, Philippe
Tetrahedron, 2005 , vol. 61, # 29 p. 7054 - 7058
反应条件
hydrogenchloride in 1,4-dioxane
参考文献
Dupont, Romain; Cotelle, Philippe
Tetrahedron Letters, 1998 , vol. 39, # 46 p. 8457 - 8460
反应条件
2: 7.9 g / acetic acid / 8 h / Heating
View Scheme
参考文献
Hoshino, Osamu; Sawaki, Shohei; Shimamura, Naomi; Onodera, Akira; Umezawa, Bunsuke
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 7 p. 2734 - 2743
反应条件
1: dioxane
2: aq. HBr
View Scheme
参考文献
CIBA-GEIGY
Patent: DE2722162 , 1977 ;
Chem.Abstr., 1978 , vol. 88, # 105559