5-甲酰基-2-甲基-1H-吡咯-3-羧酸乙酯合成路线 （共 6 条）
反应条件
sodium periodate in methanol; water
参考文献
Moreno-Vargas, Antonio J.; Robina, Inmaculada; Fernandez-Bolanos, Jose G.; Fuentes, Jose
Tetrahedron Letters, 1998 , vol. 39, # 50 p. 9271 - 9274
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Moreno-Vargas; Fernandez-Bolaos; Fuentes; Robina
Tetrahedron Asymmetry, 2001 , vol. 12, # 23 p. 3257 - 3266
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate
T=0 - 20°C; 1 h;
2: 3-(ethoxycarbonyl)-2-methylpyrrole in N,N-dimethyl-formamide
T=0 - 20°C; 1 h;
3: With water; sodium hydroxide in N,N-dimethyl-formamide
T=60°C; pH=7 - 8; 2 h; Cooling with ice;
参考文献
Jin, Yun-Zhou; Fu, Da-Xu; Ma, Nan; Li, Zhan-Cheng; Liu, Quan-Hai; Xiao, Lin; Zhang, Rong-Hua
Molecules, 2011 , vol. 16, # 11 p. 9368 - 9385
反应条件
1: aqueous acetone
2: benzene; lead (IV)-acetate
View Scheme
参考文献
Mueller; Varga
Chemische Berichte, 1939 , vol. 72, p. 1993,1998
反应条件
hydrogenchloride; diethyl ether
Erwaermen des entstandenen Imid-Hydrochlorids mit Wasser;
参考文献
Fischer; Schubert
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1926 , vol. 155, p. 109
反应条件
und Kochen des entstandenen Imid-Hydrochlorids mit Wasser,reagiert analog mit Chloracetonitril;
参考文献
Fischer; Schubert
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1926 , vol. 155, p. 109
反应条件
Erwaermen des Reaktionsprodukts;
参考文献
Fischer; Schubert
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1926 , vol. 155, p. 109
