乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
sodium cyanoborohydride; thiophenol in tert-butyl alcohol 1.75 h; Irradiation;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
AcrH(+)I(-); sodium cyanoborohydride in tetrahydrofuran 1.83333 h; UV-irradiation;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
bis(1,5-cyclooctadiene)nickel (0); NH4Br; zinc; Pybox in N,N-dimethyl acetamide T=25°C; 12 h; Inert atmosphere;
参考文献
Gong, Hegui; Andrews, R. Stephen; Zuccarello, Joseph L.; Lee, Stephen J.; Gagne, Michel R.
Organic Letters, 2009 , vol. 11, # 4 p. 879 - 882
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol T=30 - 35°C; 0.833333 h; Irradiation;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
反应条件
mercury(II) cyanide in nitromethane; benzene T=45°C; 5 h;
参考文献
Couto, Alicia; Lederkremer, Rosa M. De
Carbohydrate Research, 1984 , vol. 126, p. 313 - 320
反应条件
bis(1,5-cyclooctadiene)nickel (0); NH4Br; (R,R)-Ph-pybox; zinc in N,N-dimethyl acetamide T=25°C; 12 h; Inert atmosphere;
参考文献
Gong, Hegui; Andrews, R. Stephen; Zuccarello, Joseph L.; Lee, Stephen J.; Gagne, Michel R.
Organic Letters, 2009 , vol. 11, # 4 p. 879 - 882
反应条件
bis(1,5-cyclooctadiene)nickel (0); NH4Br; (R,R)-Ph-pybox; zinc in N,N-dimethyl acetamide T=25°C; 12 h; Inert atmosphere;
参考文献
Gong, Hegui; Andrews, R. Stephen; Zuccarello, Joseph L.; Lee, Stephen J.; Gagne, Michel R.
Organic Letters, 2009 , vol. 11, # 4 p. 879 - 882
反应条件
ammonium acetate; aluminum oxide; sulfur microwave irradiation;
参考文献
Cipolla, Laura; Redaelli, Cristina; Faria, Iris; Nicotra, Francesco
Journal of Carbohydrate Chemistry, 2006 , vol. 25, # 2-3 p. 163 - 171
反应条件
calcium sulfate; iodine; silver carbonate 1.) dichlormethane, room temp., 2 h; 2.) room temp. 30 h; Yield given. Multistep reaction;
参考文献
Takeo, Ken'ichi
Carbohydrate Research, 1980 , vol. 86, p. 151 - 157
反应条件
sodium acetate; silver trifluoromethanesulfonate; N,N,N',N'-tetramethyl-urea 1.) CH2Cl2, 1 h, -20 deg C; room temp., overnight; 2.) reflux, 20 min; Yield given. Multistep reaction;
参考文献
Takeo, Ken'ichi; Yasato, Tetsushi; Kuge, Takashi
Carbohydrate Research, 1981 , vol. 93, p. 148 - 156
