乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
1: 1.) bis(tri-n-butyltin)oxide, 2.) tetrabutylammonium bromide / 1.) toluene, reflux, 15 h, 2.) toluene, reflux, 65 h 2: 0.1 N NaOMe / methanol / 3 h / Ambient temperature View Scheme
参考文献
Ogawa, Tomoya; Nozaki, Michio; Matsui, Masanao
Tetrahedron, 1980 , vol. 36, p. 2641 - 2648
反应条件
potassium carbonate 0.5 h; Neat (no solvent)Ball milling;
参考文献
Ramrao Patil, Premanand; Ravindranathan Kartha
Green Chemistry, 2009 , vol. 11, # 7 p. 953 - 956
反应条件
1: diphenyldisulfane With zinc(II) chloride; zinc in acetonitrile T=70°C; 0.75 h; 2: 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide in acetonitrile T=70°C; 0.416667 h;
参考文献
Mukherjee, Chinmoy; Tiwari, Pallavi; Misra, Anup Kumar
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 441 - 445
反应条件
tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate in ethyl acetate T=20°C; 0.25 h;
参考文献
Larsen, Kim; Olsen, Carl Erik; Motawia, Mohammed Saddik
Carbohydrate Research, 2003 , vol. 338, # 2 p. 199 - 202
反应条件
in ethanol; chloroform 0.75 h; Heating;
参考文献
Wang, Yali; Zhang, Hong; Voelter, Wolfgang
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995 , vol. 50, # 4 p. 661 - 666
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 4 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gurudutt, Kambadoor N.; Rao, Lingamallu Jagan Mohan; Rao, Sanjay; Srinivas, Subramanian
Carbohydrate Research, 1996 , vol. 285, p. 159 - 165
反应条件
2,6-dimethylpyridine in chloroform T=20°C;
参考文献
Patel, Mitul K.; Vijayakrishnan, Balakumar; Koeppe, Julia R.; Chalker, Justin M.; Doores, Katie J.; Davis, Benjamin G.
Chemical Communications, 2010 , vol. 46, # 48 p. 9119 - 9121
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 8 h, pyridine presence, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
pyridine; benzyl alcohol zinc salt 1.) CH2Cl2, reflux, 8 h, pyridine presence, 2.) room temperature, 24 h; Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
N(Et)4ClO4 in acetonitrile Arylation; ElectrolysisAg cathode; controlled potential; Further byproducts given;
参考文献
Physical Chemistry Chemical Physics, , vol. 1, # 12 p. 2989 - 2995
