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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯硼酸
合成路线
（共 1108 条）
1282034-09-6
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
109-04-6
邻溴吡啶
+
201230-82-2
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
+
6305-18-6
(4-甲氧基苯基)(吡啶-2-基)甲酮
反应条件
caesium carbonate; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride; palladium diacetate in 1,4-dioxane T=120°C; P=37503 Torr; 45 h;
参考文献
Maerten, Eddy; Sauthier, Mathieu; Mortreux, Andre; Castanet, Yves
Tetrahedron, 2007 , vol. 63, # 3 p. 682 - 689
142-08-5
2-羟基吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
反应条件
1: 2-hydroxy-pyridine With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: (4-methoxyphenyl)-boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
2127-03-9
2,2'-二硫二吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate in 1,4-dioxane T=110°C; 12 h; Inert atmosphereSealed tubeSchlenk technique; chemoselective reaction;
参考文献
Quan, Zheng-Jun; Lv, Ying; Jing, Fu-Qiang; Jia, Xiao-Dong; Huo, Cong-De; Wang, Xi-Cun
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 325 - 332
5029-67-4
2-碘吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
反应条件
potassium carbonate in ethanol; water T=90°C; Suzuki Coupling; 0.5 h; Microwave irradiation;
参考文献
Bratt, Emma; Verho, Oscar; Johansson, Magnus J; Baeckvall, Jan-Erling
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 3946 - 3954
18438-38-5
2-甲硫基吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; acetic acid in water T=50°C; 24 h;
参考文献
Koley, Moumita; Wimmer, Laurin; Schnuerch, Michael; Mihovilovic, Marko D.
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 6 p. 1368 - 1373
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
反应条件
1.1: dichloromethane / 0.5 h / 20 °C / |Inert atmosphere 1.2: 0.25 h / 20 °C / |Inert atmosphere 2.1: triethylamine / tetrahydrofuran / 18 h / 0 - 20 °C / |Inert atmosphere 3.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol / 18 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Zhou, Bingwei; Chen, Hui; Wang, Congyang
Journal of the American Chemical Society, 2013 , vol. 135, # 4 p. 1264 - 1267
626-55-1
3-溴吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5958-02-1
3-(4-甲氧基苯基)吡啶
反应条件
potassium carbonate in isopropyl alcohol T=85 - 90°C; Suzuki-Miyaura Coupling; 24 h;
参考文献
Santra, Subhankar; Hota, Pradip Kumar; Bhattacharyya, Rangeet; Bera, Parthasarathi; Ghosh, Prasenjit; Mandal, Swadhin K.
ACS Catalysis, 2013 , vol. 3, # 12 p. 2776 - 2789
626-60-8
3-氯吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5958-02-1
3-(4-甲氧基苯基)吡啶
反应条件
NHC-Pd(II)-Im; potassium tert-butylate in water T=80°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Zhou, Xia-Xia; Shao, Li-Xiong
Synthesis, 2011 , # 19 art. no. H53711SS, p. 3138 - 3142
51581-40-9
3-吡啶氨基甲酸二乙酯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5958-02-1
3-(4-甲氧基苯基)吡啶
反应条件
1: (4-methoxyphenyl)-boronic acid T=75°C; 4 h; dehydrationvacuum; 2: 3-(N,N-diethylcarbamoyloxy)-pyridine With potassium phosphate; NiCl2(PCy3)2; PCy3∙HBF4 in o-xylene T=150°C; Suzuki-Miyaura coupling; 5 h; Inert atmosphere;
参考文献
Antoft-Finch, Aurora; Blackburn, Tom; Snieckus, Victor
Journal of the American Chemical Society, 2009 , vol. 131, # 49 p. 17750 - 17752
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