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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯硼酸
合成路线
（共 1108 条）
14508-49-7
2-氯吡嗪
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
108030-81-5
2-(4-甲氧基苯基)吡嗪
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in ethylene glycol dimethyl ether T=100°C; Suzuki coupling; 5 h;
参考文献
Nakamura, Toshio; Sato, Masakazu; Kakinuma, Hiroyuki; Miyata, Noriyuki; Taniguchi, Kazuo; Bando, Kagumi; Koda, Ayumi; Kameo, Kazuya
Journal of Medicinal Chemistry, 2003 , vol. 46, # 25 p. 5416 - 5427
290-37-9
吡嗪
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
108030-81-5
2-(4-甲氧基苯基)吡嗪
反应条件
dipotassium peroxodisulfate; Fe(acetylacetonate)2; tetrabutylammomium bromide; trifluoroacetic acid in dichloromethane; water T=20°C; 12 h;
参考文献
Singh, Parvinder Pal; Aithagani, Sravan Kumar; Yadav, Mahipal; Singh, Varun Pratap; Vishwakarma, Ram A.
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2639 - 2648
104-72-3
癸基苯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
106793-56-0
反应条件
1: phenyl-n-decane With bromine; iodine in dichloromethane T=20°C; 24 h; 2: (4-methoxyphenyl)-boronic acid With tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; toluene T=90 - 95°C; Suzuki coupling;
参考文献
Lesac, Andreja; Narancic, Sanja; Sepelj, Maja; Bruce, Duncan W.; Sunjic, Vitomir
Tetrahedron Asymmetry, 2003 , vol. 14, # 18 p. 2731 - 2737
5720-07-0
4-甲氧基苯硼酸
+
4175-77-3
2,4-二溴噻唑
→
反应条件
1078734-03-8
4-溴-2-(4-甲氧基苯基)噻唑
反应条件
potassium fluoride; [P(t-Bu)3Pd(μ-Br)]2 in tetrahydrofuran; water T=20°C; Suzuki coupling; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Proutiere, Fabien; Aufiero, Marialuisa; Schoenebeck, Franziska
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 606 - 612
5720-07-0
4-甲氧基苯硼酸
+
762-04-9
亚磷酸二乙酯
→
反应条件
3762-33-2
4-甲氧苯基磷酸二乙酯
反应条件
copper(I) oxide; 1,10-phenanthroline; N-ethyl-N,N-diisopropylamine in acetonitrile T=20°C; 24 h;
参考文献
Zhuang, Rongqiang; Xu, Jian; Cai, Zhenshi; Tang, Guo; Fang, Meijuan; Zhao, Yufen
Organic Letters, 2011 , vol. 13, # 8 p. 2110 - 2113
5720-07-0
4-甲氧基苯硼酸
→
反应条件
3393-77-9
4,4’-二甲氧基二苯硫醚
反应条件
1: (4-methoxyphenyl)-boronic acid With potassium ethylxanthate; copper(l) chloride in methanol 3 h; Inert atmosphereReflux; 2: (4-methoxyphenyl)-boronic acid With potassium hydroxide in methanol 5 h; Inert atmosphereReflux;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Synlett, 2011 , # 20 art. no. W18411ST, p. 3041 - 3045
5720-07-0
4-甲氧基苯硼酸
+
19524-06-2
4-溴吡啶盐酸盐
→
反应条件
5938-16-9
4-(4-甲氧基苯基)吡啶
反应条件
sodium salt of phosphorous acid; palladium on activated charcoal in isopropyl alcohol T=80°C; Suzuki-Miyaura coupling reaction; 3 h;
参考文献
Chemical Communications, , # 47 p. 5069 - 5071
626-64-2
4-羟基吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5938-16-9
4-(4-甲氧基苯基)吡啶
反应条件
1: 4-hydroxy-pyridine With potassium phosphate; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane; N,N-dimethyl-formamide T=100°C; 3 h; Inert atmosphere; 2: (4-methoxyphenyl)-boronic acid With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane; N,N-dimethyl-formamide T=100 - 110°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 14 p. 4038 - 4042
626-61-9
4-氯吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5938-16-9
4-(4-甲氧基苯基)吡啶
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 9 p. 1543 - 1550
1120-87-2
4-溴吡啶
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5938-16-9
4-(4-甲氧基苯基)吡啶
反应条件
8C33H27N9O3*6Pd(2+)*12NO3(1-); potassium carbonate in ethanol; water T=60°C; Suzuki-Miyaura Coupling; 10 h; Green chemistry;
参考文献
Green Chemistry, , vol. 15, # 11 p. 3150 - 3154
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