6-氧代环己烯-1-羧酸乙酯合成路线 （共 14 条）
反应条件
pyridine; benzeneselenenyl chloride in dichloromethane
T=0°C; Dehydrogenation; 1.5 h;
参考文献
Wang, Cunxiao; Gu, Xin; Yu, Marvin S.; Curran, Dennis P.
Tetrahedron, 1998 , vol. 54, # 29 p. 8355 - 8370
反应条件
titanium tetrachloride in dichloromethane
T=-40°C; 1 h;
参考文献
Funk, Raymond L.; Fitzgerald, John F.; Olmstead, Thomas A.; Para, Kim S.; Wos, John A.
Journal of the American Chemical Society, 1993 , vol. 115, # 19 p. 8849 - 8850
反应条件
dihydrogen peroxide in dichloromethane
T=0 - 20°C; Oxidation; 1 h;
参考文献
Wang, Cunxiao; Gu, Xin; Yu, Marvin S.; Curran, Dennis P.
Tetrahedron, 1998 , vol. 54, # 29 p. 8355 - 8370
反应条件
dihydrogen peroxide in dichloromethane
参考文献
Bruhn,J. et al.
Helvetica Chimica Acta, 1979 , vol. 62, p. 2630 - 2654
Full Text Show Details
Reich,H.J. et al.
Journal of the American Chemical Society, 1975 , vol. 97, # 19 p. 5434 - 5447
反应条件
dihydrogen peroxide in dichloromethane
T=0 - 20°C; 0.5 h;
参考文献
Patra, Pranab K.; Shanmugasundaram, Kandasamy; Matoba, Manabu; Nishide, Kiyoharu; Kajimoto, Tetsuya; Node, Manabu
Synthesis, 2005 , # 3 art. no. F12504SS, p. 447 - 457
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=23°C; 6.5 h;
参考文献
Duschek, Alexander; Kirsch, Stefan F.
Chemistry - A European Journal, 2009 , vol. 15, # 41 p. 10713 - 10717
反应条件
acetic acid
30 h; Ambient temperature;
参考文献
Kato, Michiharu; Kamat, Vijayendra P.; Yoshikoshi, Akira
Synthesis, 1988 , # 9 p. 699 - 701
反应条件
1: 68 percent / TiCl4; pyridine / tetrahydrofuran / 0 - 20 °C
2: 62 percent / Grubbs catalyst 2nd generation / CH2Cl2 / 4 h / Heating
View Scheme
参考文献
Toueg, Julie; Prunet, Joelle
Synlett, 2006 , # 17 p. 2807 - 2811
反应条件
toluene-4-sulfonic acid; acetone
参考文献
Brenner,J.E.
Journal of Organic Chemistry, 1961 , vol. 26, p. 22 - 27
反应条件
1: NaOMe
2: TsOH*H2O / acetone
View Scheme
参考文献
Brenner,J.E.
Journal of Organic Chemistry, 1961 , vol. 26, p. 22 - 27
