3,4-二氢-2H-吡咯合成路线 （共 44 条）
反应条件
phosphate buffer pH 7.0 T=100°C; 0.5 h;
参考文献
Hofmann, Thomas; Schieberle, Peter
Journal of Agricultural and Food Chemistry, 1998 , vol. 46, # 6 p. 2270 - 2277
反应条件
oxygen; gold in acetonitrile T=60°C; P=760.051 Torr; 40 h;
参考文献
Angelici, Robert J.
Journal of Organometallic Chemistry, 2008 , vol. 693, # 5 p. 847 - 856
反应条件
lithium Yield given. Multistep reaction;
参考文献
Scully, Frank E.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1515 - 1517
反应条件
in diethyl ether 0.5 h; Ambient temperature;
参考文献
Scully, Frank E.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1515 - 1517
参考文献
Issleib, Kurt; Doepfer, Klaus-Peter; Balszuweit, Arno
Zeitschrift fuer Chemie (Stuttgart, Germany), 1982 , vol. 22, # 6 p. 215 - 216
反应条件
potassium tert-butylate
T=80°C; P=0.001 Torr; 3 h;
参考文献
Guillemin, Jean-Claude; Denis, Jean-Marc
Tetrahedron, 1988 , vol. 44, # 14 p. 4431 - 4446
反应条件
ammonia; carbonylchlorohydridetris(triphenylphosphine) ruthenium(II); 1,1,1-tris (diphenylphosphinomethyl)ethane in toluene
T=180°C; P=36753.7 Torr; 12 h; Inert atmosphere; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2012/232292 A1, 2012 ;
Location in patent: Page/Page column 10-11 ;
反应条件
ammonia; 4,5-bis(dicyclohexylphosphinomethyl)acridine in para-xylene
T=180°C; P=38253.8 Torr; 12 h; AutoclaveInert atmosphere; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2012/232293 A1, 2012 ;
Location in patent: Page/Page column 12; 13 ;
反应条件
ammonia; 4,5-bis(dicyclohexylphosphinomethyl)acridine in tetrahydrofuran
T=180°C; P=35178.5 Torr; 12 h; AutoclaveInert atmosphere; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2012/232293 A1, 2012 ;
Location in patent: Page/Page column 12; 13 ;
反应条件
ammonia; carbonylchlorohydridetris(triphenylphosphine) ruthenium(II); 1,1,4,7,7-pentaphenyl-1,4,7-triphosphaheptane in toluene
T=155°C; P=28502.9 Torr; 12 h; Inert atmosphere; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2012/232292 A1, 2012 ;
Location in patent: Page/Page column 10; 12 ;
