反应条件
1.1: dichloro(cycloocta-1,5-diene)palladium(II); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; magnesium chloride; triethylamine / 1,4-dioxane / 80 °C / |Glovebox; |Inert atmosphere
1.2: 80 °C / |Glovebox; |Inert atmosphere
1.3: 18 h / 80 °C
2.1: hydrogenchloride / water / 1 h / 80 °C
View Scheme
参考文献
Korsager, Signe; Nielsen, Dennis U.; Taaning, Rolf H.; Lindhardt, Anders T.; Skrydstrup, Troels
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17687 - 17691
