1,4-二氢-1,4-环氧萘合成路线 (共 84 条)
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene T=25°C; Dehydrogenation; 24 h;
参考文献
European Journal of Organic Chemistry, , # 10 p. 1871 - 1874
反应条件
lanthanum; iodine in tetrahydrofuran T=25°C; 4 h;
参考文献
Kawabata, Hiroshi; Nishino, Toshiki; Nishiyama, Yutaka; Sonoda, Noboru
Tetrahedron Letters, 2002 , vol. 43, # 28 p. 4911 - 4913
反应条件
lanthanum; iodine in tetrahydrofuran T=25°C; 4 h;
参考文献
Kawabata, Hiroshi; Nishino, Toshiki; Nishiyama, Yutaka; Sonoda, Noboru
Tetrahedron Letters, 2002 , vol. 43, # 28 p. 4911 - 4913
反应条件
N-iodo-succinimide T=20°C; Ring cleavage; Cycloaddition;
参考文献
Birkett, Michael A.; Knight, David W.; Little, Paul B.; Mitchell, Michael B.
Tetrahedron, 2000 , vol. 56, # 7 p. 1013 - 1023
反应条件
1: 99 percent / mesitoic acid / toluene / 24 h / Heating 2: 99 percent / KOH / 24 h 3: 22 percent / 6 wt percent Na/Hg, NaH2PO4*H2O / dimethylformamide / 6 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 22 p. 4340 - 4345
反应条件
diethyl ether; methyllithium
参考文献
Journal of the American Chemical Society, , vol. 79, p. 2625,2627
反应条件
diethyl ether; methyllithium
参考文献
Journal of the American Chemical Society, , vol. 79, p. 2625,2627
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=0°C; 2 h;
参考文献
Effenberger, Franz; Daub, Wolfgang
Chemische Berichte, 1991 , vol. 124, # 9 p. 2113 - 2118
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=0°C; 2 h;
参考文献
Effenberger, Franz; Daub, Wolfgang
Chemische Berichte, 1991 , vol. 124, # 9 p. 2113 - 2118
反应条件
sodium amalgam in N,N-dimethyl-formamide 5 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 50, # 22 p. 4340 - 4345