N-(2-溴乙基)邻苯二甲酰亚胺合成路线 (共 110 条)
参考文献
Gabriel
Chemische Berichte, 1891 , vol. 24, p. 1117
反应条件
1: 100 percent / tetrahydrofuran / 48 h / 0 - 20 °C 2: 66 percent / TiCl4; triethylsilane / CH2Cl2; tetrahydrofuran / 1 h / -60 - 20 °C View Scheme
参考文献
Bousquet, Till; Fleury, Jean-Francois; Daich, Adam; Netchitailo, Pierre
Tetrahedron, 2006 , vol. 62, # 4 p. 706 - 715
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C;
参考文献
ChemMedChem, , vol. 9, # 4 p. 752 - 761
反应条件
1: 72 percent / NaOMe / dimethylformamide / Ambient temperature 2: N2H4*H2O / ethanol / Heating View Scheme
参考文献
Wright Jr.; Press; Chan; Marsico; Haug; Lucas; Tauber; Tomcufcik
Journal of Medicinal Chemistry, 1986 , vol. 29, # 4 p. 523 - 530
反应条件
1: 54 percent / tetrahydrofuran; cyclohexane; diethyl ether / -40 deg C, 40 min, room temp., 17 h 2: 66 percent / potassium hydroxide / H2O; methanol / 3 h / Heating View Scheme
参考文献
Wharton, Clifford J.; Wrigglesworth, Roger
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 809 - 814
反应条件
ethanol; water T=25°C; 14-taegige Einw. und folgendes Eindampfes;
参考文献
Chemische Berichte, , vol. 29, p. 2530
参考文献
Chemische Berichte, , vol. 29, p. 2530
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 11 p. 2205 - 2208
Zhurnal Organicheskoi Khimii, , vol. 21, # 11 p. 2411 - 2415
反应条件
sodium azide in N,N-dimethyl-formamide 18 h; Inert atmosphereReflux;
参考文献
Leydier, Antoine; Lin, Yi; Arrachart, Guilhem; Turgis, Raphael; Lecercle, Delphine; Favre-Reguillon, Alain; Taran, Frederic; Lemaire, Marc; Pellet-Rostaing, Stephane
Tetrahedron, 2012 , vol. 68, # 4 p. 1163 - 1170
反应条件
potassium carbonate in hydrazine hydrate; N,N-dimethyl-formamide
参考文献
Neurogen Corporation
Patent: US5972945 A1, 1999 ;
US 5972945 A