(4-甲氧基苯基)-哌啶-1-基甲酮合成路线 (共 40 条)
反应条件
tert.-butylhydroperoxide in decane; acetonitrile
T=70°C; 6 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian; Bhat, Vikram; Rawal, Viresh
Organic Syntheses, 2010 , vol. 87, p. 1 - 7
反应条件
tert.-butylhydroperoxide; potassium carbonate in tetrahydrofuran
T=80°C; 12 h; Sealed tube;
参考文献
Zhao, Qiong; Li, Hongji; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6772 - 6779
反应条件
potassium carbonate; 1,1'-bis(diphenylphosphino)ferrocene; [(Pd(.mu.-Cl)(.kappa.(2)-P,C-P(OC6H2-2,4-tBu2)(OC6H3-2,4-tBu2)2))2] in 1,4-dioxane
T=120°C; P=7500.6 Torr;
参考文献
Fairlamb, Ian J. S.; Grant, Stephanie; McCormack, Peter; Whittall, John
Dalton Transactions, 2007 , # 8 p. 859 - 865
反应条件
N-iodo-succinimide; oxygen; copper(I) bromide in toluene
T=20°C;
参考文献
Zhang, Juan; Wei, Ying; Lin, Shaoxia; Liang, Fushun; Liu, Pengjun
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 46 p. 9237 - 9242
反应条件
in dichloromethane
T=5°C; 0.333333 h;
参考文献
Ishihara, Hideharu; Muto, Shinya; Kato, Shinzi
Synthesis, 1986 , # 1 p. 128 - 130
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=65°C; 12 h;
参考文献
Lindsay, Charles M.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 569 - 574
反应条件
in diethyl ether
T=0°C; 1 h;
参考文献
Kimura, Mitsutoshi; Iwata, Akiyuki; Itoh, Masahiro; Yamada, Kazuki; Kimura, Tsutomu; Sugiura, Noriyuki; Ishida, Masaru; Kato, Shinzi
Helvetica Chimica Acta, 2006 , vol. 89, # 4 p. 747 - 783
反应条件
mercury dibromide in toluene
12 h; Heating;
参考文献
Fujiwara, Shin-Ichi; Ogawa, Akiya; Kambe, Nobuaki; Ryu, Ilhyong; Sonoda, Noboru
Tetrahedron Letters, 1988 , vol. 29, # 47 p. 6121 - 6124
反应条件
pyridine; tris-(dibenzylideneacetone)dipalladium(0); cis-1,3-bis[(di-tert-butylphosphino)methyl]cyclohexane in dichloromethane
T=45°C; P=750.075 Torr; 14 h; Inert atmosphere; chemoselective reaction;
参考文献
De La Fuente, Veronica; Godard, Cyril; Claver, Carmen; Castillon, Sergio
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 10 p. 1971 - 1979
反应条件
tert.-butylhydroperoxide; potassium carbonate in tetrahydrofuran
T=80°C; 12 h; Sealed tube;
参考文献
Zhao, Qiong; Li, Hongji; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6772 - 6779