(4-甲氧基苯基)-哌啶-1-基甲酮合成路线 (共 40 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Heating;
参考文献
Lindsay, Charles M.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 569 - 574
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
T=60°C; P=750.075 Torr; 14 h; Microreactor; chemoselective reaction;
参考文献
De La Fuente, Veronica; Godard, Cyril; Zangrando, Ennio; Claver, Carmen; Castillon, Sergio
Chemical Communications, 2012 , vol. 48, # 11 p. 1695 - 1697
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Heating;
参考文献
Lindsay, Charles M.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 569 - 574
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696
反应条件
1: ethyl tribromoacetate; triphenylphosphine / CH2Cl2 / 3 h / 20 °C
2: Et3N / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696
反应条件
1: triethylamine / diethyl ether
2: water; dimethyl sulfoxide / 25 °C
View Scheme
参考文献
Im, Li-Ra; Jeon, Sang-Eun; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 4 p. 1153 - 1157
反应条件
in water; dimethyl sulfoxide; acetonitrile
T=25°C; Kinetics;
参考文献
Jeon, Seong Hoon; Kim, Hyun Soo; Han, Young Joon; Kim, Min-Young; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2014 , vol. 35, # 2 p. 471 - 476
反应条件
in tetrahydrofuran
12 h; Ambient temperature;
参考文献
Pri-Bar, Ilan; Alper, Howard
Journal of Organic Chemistry, 1989 , vol. 54, # 1 p. 36 - 38
反应条件
hydrogenchloride in dimethyl sulfoxide; acetonitrile
T=25°C; Substitution; Kinetics;
参考文献
Um, Ik-Hwan; Min, Ji-Sook; Ahn, Jung-Ae; Hahn, Hyun-Joo
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5659 - 5663
反应条件
water in dimethyl sulfoxide
T=25°C; aminolysis; Kinetics;
参考文献
Um, Ik-Hwan; Min, Ji-Sook; Lee, Hye-Won
Canadian Journal of Chemistry, 1999 , vol. 77, # 5-6 p. 659 - 666