2,4,5-三甲基苯甲醛合成路线 (共 57 条)
反应条件
hydrogen fluoride; boron trifluoride T=-20°C; P=15001.5 Torr; 0.416667 h;
参考文献
MITSUBISHI GAS CHEMICAL COMPANY, INC.
Patent: EP1380560 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
zink cyanide; aluminium trichloride; benzene T=40 - 45°C; Einleiten von HCl und Behandeln des Reaktionsgemisches mit wss. HCl;
参考文献
Journal of the American Chemical Society, , vol. 58, p. 629,634
Journal of Organic Chemistry, , vol. 8, p. 147,148
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid T=25°C; P=760 Torr; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 62, # 20 p. 6810 - 6813
反应条件
pyridinium chlorochromate in acetonitrile 4 h; Heating;
参考文献
Hosseinzadeh, Rahman; Tajbakhsh, Mahmood; Vahedi, Hossein
Synlett, 2005 , # 18 art. no. D19905ST, p. 2769 - 2770
反应条件
dinitrogen tetraoxide in dichloromethane T=25°C; 1.5 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 12 p. 3314 - 3325
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3846 - 3850
反应条件
2-hydroxy-1,3-isoindolinedione; xanthone powder; oxygen; anhydrous tetramethylammonium chloride in acetonitrile T=60°C; P=3750.38 Torr; 3 h; Autoclave;
参考文献
Tetrahedron Letters, , vol. 50, # 15 p. 1677 - 1680
反应条件
air; copper diacetate; anhydrous cobalt diacetate; acetic acid; sodium bromide T=150°C; P=15200 Torr; 1 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 9 p. 2724 - 2727
反应条件
sulfuric acid; water; oxygen; [Acr+-Mes]ClO4- in acetonitrile 1.33333 h; Irradiation; Quantum yield; Reagent/catalyst;
参考文献
Chemical Communications, , vol. 46, # 4 p. 601 - 603
反应条件
air; copper diacetate; anhydrous cobalt diacetate; sodium bromide T=150°C; P=15200 Torr; 1 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 9 p. 2724 - 2727