phosphorus tribromide in diethyl ether
T=20°C; 0.166667 h;
参考文献
Zhi, Lin; Tegley, Christopher M.; Pio, Barbara; Edwards, James P.; Motamedi, Mehrnouch; Jones, Todd K.; Marschke, Keith B.; Mais, Dale E.; Risek, Boris; Schrader, William T.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 19 p. 4104 - 4112
1.1: n-BuLi / diethyl ether; hexane / 4 h / Heating
1.2: 33 percent / diethyl ether; hexane / 1 h / 20 °C
2.1: 94 percent / PBr3 / diethyl ether / 0.17 h / 20 °C
View Scheme
参考文献
Zhi, Lin; Tegley, Christopher M.; Pio, Barbara; Edwards, James P.; Motamedi, Mehrnouch; Jones, Todd K.; Marschke, Keith B.; Mais, Dale E.; Risek, Boris; Schrader, William T.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 19 p. 4104 - 4112