反-3-甲氧基丙烯酸甲酯合成路线 （共 30 条）
反应条件
1: With sodium hydrogencarbonate; triphenylphosphine; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=150°C; Heck reaction; 20 h; 2: With hydrogenchloride in dichloromethane; water T=25°C;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
hydrogenchloride in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; chloroform-d1; N,N-dimethyl-formamide
参考文献
Ishihara Sangyo Kaisha Ltd.
Patent: US5708175 A1, 1998 ;
参考文献
Journal of Organic Chemistry, , vol. 58, # 16 p. 4211 - 4218
反应条件
ozone T=-70°C; other substrates, other solvents, also with CD3OD; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 58, # 16 p. 4211 - 4218
反应条件
in toluene T=200°C; Diels-Alder Cycloaddition; 16 h; Inert atmosphereSealed tube;
参考文献
Lee, Jennifer J.; Kraus, George A.
Green Chemistry, 2014 , vol. 16, # 4 p. 2111 - 2116
反应条件
N-iodo-succinimide in dichloromethane; acetic acid T=20°C; 24 h;
参考文献
Coleman, Robert S.; Lu, Xiaoling
Chemical Communications, 2006 , # 4 p. 423 - 425
反应条件
1: With sodium hydrogencarbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=150°C; Heck reaction; 20 h; 2: With hydrogenchloride in tetrahydrofuran T=25°C; Further stages.;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
trichlorophosphate in acetic acid T=25°C; 18 h;
参考文献
Tetrahedron Letters, , vol. 46, # 22 p. 3875 - 3878
反应条件
lithium diisopropyl amide
1.) THF, -90 degC.,2 min, 2.) THF, -90 degC, 60 min.; Yield given. Multistep reaction;
参考文献
Miyata, Okiko; Schmidt, Richard R.
Tetrahedron Letters, 1982 , vol. 23, # 17 p. 1793 - 1796
反应条件
triethylamine in ethanol
5 h; Heating;
参考文献
Loeber, Stefan; Huebner, Harald; Gmeiner, Peter
Bioorganic & Medicinal Chemistry Letters, 1999 , vol. 9, # 1 p. 97 - 102
