1-苯基-1,2-丙二酮合成路线 （共 223 条）
反应条件
1: 14 percent Spectr. / 0.50 M aq. NaOH, aq. KCl, aq. NaOCl / methanol / 3 h / Ambient temperature 2: 5percent H2SO4 / 1.5 h / Heating View Scheme
参考文献
Guthrie, J. Peter; Cossar, John; Lu, Jinqiao
Canadian Journal of Chemistry, 1991 , vol. 69, # 12 p. 1904 - 1908
反应条件
in tetrahydrofuran; hexane Ambient temperature; Title compound not separated from byproducts;
参考文献
Katritzky, Alan R.; Jiang, Jinlong; Steel, Peter J.
Journal of Organic Chemistry, 1994 , vol. 59, # 16 p. 4551 - 4555
反应条件
water; palladium Hydrogenation;
参考文献
Skita; Keil; Baesler
Chemische Berichte, 1933 , vol. 66, p. 865
Full Text Show Details
Knoll A.G.
Patent: DE634002 , 1930 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 23, p. 481
反应条件
sodium hydroxide; sodium hypochlorite; potassium chloride in methanol 3 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 12 p. 1904 - 1908
反应条件
1.1: tetrahydrofuran / 0.5 h / 25 °C 1.2: 97 percent / tetrahydrofuran / 0.5 h / 25 °C 2.1: 83 percent / FeCl3 / tetrahydrofuran / 0 °C View Scheme
参考文献
Ukai; Oshima; Matsubara
Journal of the American Chemical Society, 2000 , vol. 122, # 48 p. 12047 - 12048
反应条件
sodium hydroxide; water; potassium hexacyanoferrate(III) man extrahiert mit Benzol, verdunstet die Bezolloesung, waescht den Rueckstand mit Aether und erwaermt ihn mit einem Gemisch von Alkohol und maessig verd. Salpetersaeure;
参考文献
Mueller; v. Pechmann
Chemische Berichte, 1889 , vol. 22, p. 2131
反应条件
sodium hydroxide; sodium hypochlorite; potassium chloride in methanol 3 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 12 p. 1904 - 1908
反应条件
[Rh(NCMe)2(cod)][BF4] in tetrahydrofuran T=60°C; 20 h; Title compound not separated from byproducts;
参考文献
Oi, Shuichi; Moro, Mitsutoshi; Fukuhara, Hiroe; Kawanishi, Takanori; Inoue, Yoshio
Tetrahedron, 2003 , vol. 59, # 24 p. 4351 - 4361
反应条件
sodium hydroxide; sodium hypochlorite; potassium chloride in methanol 3 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 12 p. 1904 - 1908
参考文献
de la Morena; Marquez; Archilla
Anales de la Real Sociedad Espanola de Fisica y Quimica, Serie B: Quimica, 1958 , vol. 54, p. 715,717
