双(三甲基硅基)过氧化物合成路线 （共 69 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane
参考文献
Halbert, Stacie Marie; Michaud, Evelyne; Thompson, Scott Kevin; Veber, Daniel Frank
Patent: US2002/49316 A1, 2002 ;
反应条件
in tetrahydrofuran; diethyl ether T=0°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
in tetrahydrofuran; diethyl ether T=0°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
in n-heptane T=-20°C; addition of lithium tert- butoxide or lithium trimethylsilanolate; KineticsMechanism;
参考文献
Baryshnikov, Yu. N.; Kurskii, Yu. A.; Kaloshina, N. N.; Vesnovskaya, G. I.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2288 - 2292,2037 - 2040
反应条件
in various solvent(s) T=343°C; E(activ.); Rate constantMechanismProduct distribution;
参考文献
Gorbatov, V. V.; Yablokova, N. V.; Aleksandrov, Yu. A.; Ivanov, V. I.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1752 - 1755,1576 - 1578
反应条件
lithium bromide in diethyl ether T=0°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78°C; 2 h; alkylation of other heteroaryl alkyl metals;
参考文献
Tetrahedron, , vol. 46, p. 4031 - 4038
反应条件
(i) tBuLi, THF, ether, pentane, (ii) /BRN= 1739972/; Multistep reaction;
参考文献
Neumann,H.; Seebach,D.
Chemische Berichte, 1978 , vol. 111, p. 2785 - 2812
反应条件
n-butyllithium 1.) -60 grad C 30 min, rt 3 h, ether, hexane, 2) -50 grad C, then rt overnight; Multistep reaction. Title compound not separated from byproducts;
参考文献
Ricci, Alfredo; Innocenti, Alessandro Degl'; Ancillotti, Monica; Seconi, Giancarlo; Dembech, Pasquale
Tetrahedron Letters, 1986 , vol. 27, # 49 p. 5985 - 5988
