trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, aryl halide and tributylstannyl chloride added simultaneously in MeCN at room temp., stirred for 1 h at 50°C;
参考文献
Gosmini, Corinne; Perichon, Jacques
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 2 p. 216 - 217
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide in acetonitrile CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, reacted with aryl bromide, tributylstannyl chloride added at room temp., stirred for 30 min; hydrolyzed with NH4Cl, extd. (Et2O), chromd. (silica gel, pentane);
参考文献
Gosmini, Corinne; Perichon, Jacques
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 2 p. 216 - 217
