D-alpha-生育酚醋酸酯合成路线 （共 18 条）
反应条件
hydrogenchloride; sulfuric acid; oxalic acid; acetic anhydride in 1,2,3,4-tetrahydro-naphthalene; n-heptane
参考文献
BASF Aktiengesellschaft
Patent: US5468883 A1, 1995 ;
反应条件
indium trifluoromethanesulfonate T=25 - 32°C; 4.66667 h; Product distribution / selectivity;
参考文献
DSM IP ASSETS B.V.
Patent: WO2005/54223 A2, 2005 ;
Location in patent: Page/Page column 40 ;
参考文献
BASF Aktiengesellschaft
Patent: US5468883 A1, 1995 ;
反应条件
C30H42IrNOP(1+)*C32H12BF24(1-); hydrogen in dichloromethane T=20°C; P=37503.8 Torr; 2 h; optical yield given as percent destereoselective reaction;
参考文献
Chemistry - An Asian Journal, , vol. 6, # 2 p. 599 - 606
反应条件
1: C39H55ClO5 With lithium aluminium tetrahydride in tetrahydrofuran 18 h; Reflux; 2: acetic anhydride in pyridine T=25°C; 4 h; 3: With chiral Iridium catalyst; hydrogen in dichloromethane T=25°C; P=37503.8 Torr; 3 h;
参考文献
European Journal of Organic Chemistry, , # 13 p. 2069 - 2076
参考文献
Journal of the Chemical Society, , p. 3100
Journal of the American Chemical Society, , vol. 64, p. 1487
参考文献
WO2006/18310 A2, ;
Page/Page column 21 ;
反应条件
1: H2 / Pd/C 2: pyridine View Scheme
参考文献
Helvetica Chimica Acta, , vol. 64, # 4 p. 1158 - 1173
反应条件
1: 93 percent / Li2CuCl4 2: H2 / Pd/C 3: pyridine View Scheme
参考文献
Helvetica Chimica Acta, , vol. 64, # 4 p. 1158 - 1173
