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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴代萘
合成路线
（共 389 条）
580-13-2
2-溴代萘
+
7439-95-4
镁
→
反应条件
21473-01-8
2-萘基溴化镁
反应条件
in tetrahydrofuran 2 h; Heating / reflux;
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2007/37983 A1, 2007 ;
Location in patent: Page/Page column 15 ;
580-13-2
2-溴代萘
→
反应条件
194-59-2
7H-二苯并咔唑
+
4488-22-6
[1,1’-联萘]-2,2’-二胺
反应条件
1: [HP(t-Bu3)]BF4; palladium diacetate; caesium carbonate / N,N-dimethyl-formamide / 5 h / 100 °C / Inert atmosphere 2: sulfuric acid; acetic acid / 0.08 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 455 - 457
580-13-2
2-溴代萘
+
201230-82-2
→
反应条件
2243-82-5
萘-2-甲酰胺
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; ammonia; palladium diacetate in 1,4-dioxane T=100°C; P=1500.15 Torr; 16 h;
参考文献
Chemistry - An Asian Journal, , vol. 5, # 10 p. 2168 - 2172
580-13-2
2-溴代萘
→
反应条件
2018-90-8
萘-2-甲胺
反应条件
1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; sodium carbonate; bis(dibenzylideneacetone)-palladium(0) / 1,4-dioxane; water / 36 h / Reflux 2: ethylenediamine / 1,4-dioxane; propan-1-ol; water / 24 h / Reflux View Scheme
参考文献
Murai, Norio; Miyano, Masayuki; Yonaga, Masahiro; Tanaka, Keigo
Organic Letters, 2012 , vol. 14, # 11 p. 2818 - 2821
580-13-2
2-溴代萘
→
反应条件
2243-57-4
2-萘肼
反应条件
potassium phosphate; copper(l) iodide; hydrazine hydrate T=120°C; 6 h; Sealed tubeInert atmosphere;
参考文献
Chen, Junmin; Zhang, Yimin; Hao, Wenyan; Zhang, Rongli; Yi, Fei
Tetrahedron, 2013 , vol. 69, # 2 p. 613 - 617
→
反应条件
22082-99-1
2-(4-溴苯基)萘
反应条件
hydrogenchloride; tert.-butyl lithium; sodium thiosulfate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; pentane
参考文献
Bristol-Myers Squibb Company
Patent: US5470845 A1, 1995 ;
580-13-2
2-溴代萘
→
反应条件
22082-99-1
2-(4-溴苯基)萘
反应条件
1.1: Mg; I2 / tetrahydrofuran / 14 h / Heating 1.2: tetrahydrofuran / -78 - 20 °C 2.1: 6.2 g / aq. HCl / tetrahydrofuran / 2 h / 20 °C 3.1: 79 percent / Pd(PPh3)4; Ba(OH)2*8H2O / H2O; dioxane / 24 h / Heating View Scheme
参考文献
Wipf, Peter; Jung, Jae-Kyu
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6319 - 6337
3054-95-3
+
580-13-2
2-溴代萘
→
反应条件
112598-96-6
+
20884-05-3
反应条件
1: With C16H18Cl2N2O4Pd2; potassium chloride; tetra-n-butylammonium acetate; potassium carbonate in N,N-dimethyl acetamide T=120°C; Heck reaction; 3.5 h; 2: With hydrogenchloride in water; ethyl acetate T=20°C; chemoselective reaction;
参考文献
Alacid, Emilio; Najera, Carmen
European Journal of Organic Chemistry, 2008 , # 18 p. 3102 - 3106
3054-95-3
+
580-13-2
2-溴代萘
→
反应条件
91-20-3
+
112598-96-6
反应条件
1: With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); sodium acetate in 1-methyl-pyrrolidin-2-one T=140°C; 6 h; 2: With hydrogenchloride; water in 1-methyl-pyrrolidin-2-one
参考文献
Noel, Sebastien; Djakovitch, Laurent; Pinel, Catherine
Tetrahedron Letters, 2006 , vol. 47, # 23 p. 3839 - 3842
141-32-2
+
580-13-2
2-溴代萘
→
反应条件
124182-61-2
反应条件
sodium carbonate; silica supported Pd-NHC in N,N-dimethyl-formamide T=140°C; Mizoroki-Heck reaction; 20 h;
参考文献
Aksin, Oezge; Tuerkmen, Hayati; Artok, Levent; Cetinkaya, Bekir; Ni, Chaoying; Bueyuekguengoer, Orhan; Oezkal, Erhan
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 3027 - 3036
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