联苯-2,2-二羧酸二甲酯合成路线 （共 68 条）
反应条件
carbon monoxide; copper; 1-iodo-propane; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=50°C; P=760 Torr; 22 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
1: With copper; tris(dibenzylideneacetone)dipalladium (0) in dimethyl sulfoxide
T=90°C; 2.5 h;
2: With hydrogen; palladium on activated charcoal in methanol
T=18°C; P=760 Torr; 0.75 h;
参考文献
Banwell, Martin G.; Lupton, David W.; Ma, Xinghua; Renner, Jens; Sydnes, Magne O.
Organic Letters, 2004 , vol. 6, # 16 p. 2741 - 2744
反应条件
copper; tris(dibenzylideneacetone)dipalladium (0) in dimethyl sulfoxide
T=90°C; 2.5 h; Title compound not separated from byproducts;
参考文献
Banwell, Martin G.; Lupton, David W.; Ma, Xinghua; Renner, Jens; Sydnes, Magne O.
Organic Letters, 2004 , vol. 6, # 16 p. 2741 - 2744
反应条件
copper trifluoromethanesulfonate in acetonitrile
T=0 - 20°C; 26 h;
参考文献
Cepanec, Ivica; Litvic, Mladen; Udikovic, Josipa; Pogorelic, Ivan; Lovric, Marija
Tetrahedron, 2007 , vol. 63, # 25 p. 5614 - 5621
反应条件
copper trifluoromethanesulfonate in acetonitrile
T=20°C; 23 h;
参考文献
Cepanec, Ivica; Litvic, Mladen; Udikovic, Josipa; Pogorelic, Ivan; Lovric, Marija
Tetrahedron, 2007 , vol. 63, # 25 p. 5614 - 5621
反应条件
carbon monoxide; methyl 2-iodobenzoate; copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
P=760 Torr; -78 deg C, 2h; room temp., 1 h; 60 deg C, 6 h; Further byproducts given;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
carbon monoxide; copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
P=760 Torr; -78 deg C, 2h; room temp., 1 h; 60 deg C, 6 h; Further byproducts given;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=110°C; 1 h;
参考文献
Kim, Hoo Sook; Gowrisankar, Saravanan; Kim, Eun Sun; Kim, Jae Nyoung
Tetrahedron Letters, 2008 , vol. 49, # 46 p. 6569 - 6572
反应条件
copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
P=760 Torr; -78 deg C, 2h; room temp., 1 h; 60 deg C, 6 h; Further byproducts given;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
1: 81 percent / pyridine
2: NiCl2(PPh3)2, Zn, Et4NI / tetrahydrofuran / 1.) r.t., 5 min, 2.) 67 deg C, 24 h
View Scheme
参考文献
Percec, Virgil; Bae, Jin-Young; Zhao, Mingyang; Hill, Dale H.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 176 - 185
