1-苯基-1,4-戊二酮合成路线 (共 177 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Heating;
参考文献
Echavarren, Antonio M.; Perez, Marta; Castano, Ana M.; Cuerva, Juan M.
Journal of Organic Chemistry, 1994 , vol. 59, # 15 p. 4179 - 4185
反应条件
lithium aluminium tetrahydride; antimony trichloride in tetrahydrofuran T=0°C; 4 h;
参考文献
Sayama, Shinsei; Inamura, Yutaka
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 1 p. 306 - 308
反应条件
tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran T=50°C; 2 h;
参考文献
Shirakawa; Yamamoto; Nakao; Tsuchimoto; Hiyama
Chemical Communications, 2001 , # 19 p. 1926 - 1927
反应条件
1: chlorobenzene With chloro-trimethyl-silane; zinc in tetrahydrofuran T=40°C; 4 h; 2: carbon monoxide; methyl vinyl ketone With tetrakis(triphenylphosphine) palladium(0); chloro-trimethyl-silane; lithium chloride in tetrahydrofuran T=30°C; P=760 Torr; 0.583333 h;
参考文献
Yuguchi, Motoki; Tokuda, Masao; Orito, Kazuhiko
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 908 - 914
反应条件
1: acetone With pyrrolidinium hydrochloride in water; N,N-dimethyl-formamide T=55°C; 2: styrene With manganese(IV) oxide; Cu(ClO4)2*6H2O in water; N,N-dimethyl-formamide T=55°C; 72 h;
参考文献
Xie, Jin; Huang, Zhi-Zhen
Chemical Communications, 2010 , vol. 46, # 11 p. 1947 - 1949
反应条件
1: With potassium carbonate in water T=20°C; Michael addition; 3 h; 2: With dihydrogen peroxide; potassium carbonate in water T=20°C; Nef reaction;
参考文献
Ballini, Roberto; Barboni, Luciano; Giarlo, Guido
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 9173 - 9176
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in dichloromethane T=0°C; 0.5 h; 2: 1-phenylbutane-1,3-dione in dichloromethane T=20°C; 5 h;
参考文献
Xue, Song; Li, Le-Zhen; Liu, Yong-Kang; Guo, Qing-Xiang
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 215 - 218
反应条件
RhH(CO)(triphenylphosphine)3 in methanol T=80°C; P=30002.4 Torr; 18 h;
参考文献
Chochois, Helene; Sauthier, Mathieu; Maerten, Eddy; Castanet, Yves; Mortreux, Andre
Tetrahedron, 2006 , vol. 62, # 50 p. 11740 - 11746
反应条件
hydrogenchloride; sodium iodide in acetone T=0°C; 0.0833333 h;
参考文献
Mayring, Lothar; Severin, Theodor
Chemische Berichte, 1981 , vol. 114, p. 3863 - 3877
反应条件
sodium tetrahydroborate; antimony(III)tribromide in tetrahydrofuran; dimethyl sulfoxide T=0 - 22°C;
参考文献
Sayama, Shinsei; Inamura, Yutaka
Chemistry Letters, 1996 , # 8 p. 633 - 634