反应条件
in methanol; water a soln. of bipy and K2C2O4 in 1:1 water-MeOH was added under inert atm. to a soln. of Ru-complex in hot water, mixt. was refluxed for 24 h; according to the adapted procedure by C. F. Liu, N. C. Liu and J. Bailar, Inorg. Chem., 1964, 1197; filtd., evapd., residue was recrystd. from MeOH; (1)H NMR spectral data;
参考文献
Kuimova, Marina K.; Mel'nikov, Michael Ya.; Weinstein, Julia A.; George, Michael W.
Journal of the Chemical Society. Dalton Transactions, 2002 , # 14 p. 2857 - 2861
