Mascarelli; Gatti
Gazzetta Chimica Italiana, 1931 , vol. 61, p. 782,788
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1931 , vol. <6> 13, p. 887,890
1.1: tetrakis(triphenylphosphine)palladium; K3PO4 / dimethylformamide / 48 h / 100 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C 2.2: 877 mg / tetrahydrofuran; hexane / a) -78 deg C, 15 min, b) RT, 20 h View Scheme
参考文献
Wolfe, John P.; Singer, Robert A.; Yang, Bryant H.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1999 , vol. 121, # 41 p. 9550 - 9561
1.1: 1.57 g / tetrakis(triphenylphosphine)palladium; Na2CO3 / 1,2-dimethoxy-ethane; H2O; ethanol / 42 h / 90 °C 2.1: n-BuLi / tetrahydrofuran / 1.17 h / -78 °C 2.2: 65 percent / tetrahydrofuran / a) -78 deg C, 20 min, b) 0 deg C, 20 min, c) RT, 18 h View Scheme
参考文献
Wolfe, John P.; Singer, Robert A.; Yang, Bryant H.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1999 , vol. 121, # 41 p. 9550 - 9561
