反应条件
1.1: copper(l) iodide; Pd2(PPh3)2Cl2; diethylamine / 20 °C / Inert atmosphere
2.1: tris-(dibenzylideneacetone)dipalladium(0); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene / toluene / 0.03 h / Inert atmosphere
2.2: 0.75 h / 130 °C / Inert atmosphere; Microwave irradiation
3.1: caesium carbonate / toluene / 0.25 h / 130 °C / Inert atmosphere; Microwave irradiation
View Scheme
参考文献
Guilarte, Veronica; Fernandez-Rodriguez, Manuel A.; Garcia-Garcia, Patricia; Hernando, Elsa; Sanz, Roberto
Organic Letters, 2011 , vol. 13, # 19 p. 5100 - 5103