反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / 18 h / 20 °C / Inert atmosphere
2: potassium hydroxide / methanol / 18 h / 20 °C / Inert atmosphere
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / 18 h / 20 °C / Inert atmosphere
4: diisobutylaluminium hydride / hexane / 18 h / Cooling with ice; Reflux
View Scheme
参考文献
Yoshida, Kengo; Furuyama, Taniyuki; Wang, Chao; Muranaka, Atsuya; Hashizume, Daisuke; Yasuike, Shuji; Uchiyama, Masanobu
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 729 - 732