2-烯丙基-4-甲氧基苯酚合成路线 （共 28 条）
反应条件
boron tribromide in dichloromethane
T=-40°C; 0.05 h;
参考文献
Punna, Sreenivas; Meunier, Stephane; Finn
Organic Letters, 2004 , vol. 6, # 16 p. 2777 - 2779
反应条件
tin(IV) chloride in dichloromethane
T=20°C; 2 h;
参考文献
Sarkar, Debayan; Venkateswaran, Ramanathapuram V.
Synlett, 2008 , # 5 p. 653 - 654
反应条件
[Ir(1,5-cyclooctadiene)(CH3CN)2]PF6 in toluene
T=0°C; 15 h;
参考文献
Tsukada, Naofumi; Yagura, Yasushige; Sato, Tetsuo; Inoue, Yoshio
Synlett, 2003 , # 10 p. 1431 - 1434
反应条件
1: 86 percent / K2CO3 / acetonitrile / 3 h / Heating
2: 82 percent / MgCl2; 1-butyl-2,3-(trimethylene)imidazolium bistriflylimide / 0.04 h / 200 °C / microwave irradiation
View Scheme
参考文献
Lin, Yung-Lun; Cheng, Jen-Yen; Chu, Yen-Ho
Tetrahedron, 2007 , vol. 63, # 45 p. 10949 - 10957
参考文献
Baker, Jillian G.; Fischer, Peter M.; Fromont, Christophe; Gardiner, Sheila M.; Hill, Stephen J.; Jadhav, Gopal; Kellam, Barrie; Mistry, Shailesh; Woolard, Jeanette
Patent: US2014/94493 A1, 2014 ;
Location in patent: Page/Page column ;
反应条件
diisobutylaluminium hydride in hexane; dichloromethane
T=20°C; Reduction; Claisen rearrangement; 24 h; Title compound not separated from byproducts;
参考文献
Sharma; Ilangovan; Sreenivas, Punna; Mahalingam
Synlett, 2000 , # 5 p. 615 - 618
反应条件
ytterbium(III) triflate in acetonitrile
Substitution; Claisen rearrangement; 60 h; Heating;
参考文献
Sharma; Ilangovan; Sreenivas, Punna; Mahalingam
Synlett, 2000 , # 5 p. 615 - 618
反应条件
1: potassium carbonate / acetone
2: potassium carbonate / acetone
3: 10 h / 180 °C
View Scheme
参考文献
Akhtar, Yasmin; Yu, Yang; Isman, Murray B.; Plettner, Erika
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 8 p. 4983 - 4991
反应条件
N-n-heptylpyridinium bromide
T=200°C; Claisen rearrangement; 4 h; Inert atmosphere;
参考文献
Katkevica; Zicmanis; Mekss
Chemistry of Heterocyclic Compounds, 2010 , vol. 46, # 2 p. 158 - 169
反应条件
1: With potassium carbonate in acetone
8 h; RefluxInert atmosphereSchlenk technique;
2: in 1,2-dichloro-benzene; acetone
6 h; RefluxInert atmosphereSchlenk technique;
参考文献
Majumdar; Nandi, Raj Kumar; Ganai, Sintu
Tetrahedron Letters, 2014 , vol. 55, # 6 p. 1247 - 1250
