反应条件
1: 1-bromo-1-phenyl-ethane With chloro-trimethyl-silane; ethylene dibromide; lithium chloride; zinc in tetrahydrofuran T=50°C; 6 h; Inert atmosphere; 2: 4-methoxybenzenediazonium tetrafluoroborate With zinc dibromide in tetrahydrofuran T=-60 - 25°C; Inert atmosphere; 3: With chloro-trimethyl-silane in tetrahydrofuran T=125°C; 1.5 h; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Haag, Benjamin A.; Zhang, Zhi-Guang; Li, Jin-Shan; Knochel, Paul
Angewandte Chemie - International Edition, 2010 , vol. 49, # 49 p. 9513 - 9516