1: (benzyl)-triphenylphosphonium chloride With n-butyllithium in tetrahydrofuran; hexane T=0°C; Wittig type reaction; 2: 3-Methyl-hydroxymethyl benzene With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride in tetrahydrofuran; hexane Wittig type reaction; 8 h; Inert atmosphereReflux; optical yield given as percent de;
参考文献
Alonso, Francisco; Riente, Paola; Yus, Miguel
European Journal of Organic Chemistry, 2009 , # 34 p. 6034 - 6042
4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride in tetrahydrofuran Wittig type olefination reaction; 8 h; RefluxInert atmosphere; optical yield given as percent de;
参考文献
Alonso, Francisco; Riente, Paola; Yus, Miguel
Synlett, 2009 , # 10 p. 1579 - 1582