双(硫代苯甲酰基)二硫化物合成路线 (共 25 条)
参考文献
Journal of the American Chemical Society, , vol. 48, p. 2717
反应条件
NaCH3COO; hydrochloric acid in water to aq. soln. of Na2MoO4*2H2O, (NEt2H2)(S2CPh), and MeCO2Na added HCl (1.0 M) dropwise with stirring at room temp.; ppt. filtered off, washed with water and methanol, dried in vac., chromd. (SiO2, CS2), orange fraction evapd. in vac., recrystd. from CH2Cl2-light petroleum; elem. anal.;
参考文献
Tatsumisago, Masahiro; Matsubayashi, Gen-etsu; Tanaka, Toshio; Nishigaki, Satoshi; Nakatsu, Kazumi
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1982 , p. 121 - 128
参考文献
Kato, Shinzi; Goto, Masahisa; Hattori, Rikizoh; Nishiwaki, Koh-ichi; Mizuta, Masateru; Ishida, Masaru
Chemische Berichte, 1985 , vol. 118, # 4 p. 1668 - 1683
反应条件
nachf. Behandeln mit Benzoylchlorid;
参考文献
Journal of the American Chemical Society, , vol. 48, p. 2717
参考文献
Chemische Berichte, , vol. 39, p. 3224
反应条件
in ethyl acetate T=70°C; 48 h;
参考文献
Commonwealth Scientific and Industrial Research Organisation
Patent: EP1149075 B1, 2008 ;
Location in patent: Page/Page column 15 ;
参考文献
Fromm; Schmoldt
Chemische Berichte, 1907 , vol. 40, p. 2869
反应条件
in ethyl acetate 18 h; Heating;
参考文献
Tetrahedron Letters, , vol. 40, # 12 p. 2435 - 2438
反应条件
in ethyl acetate T=85°C; 12 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 38 p. 10656 - 10658
反应条件
in ethyl acetate T=80°C; 20 h; Inert atmosphere;
参考文献
Canadian Journal of Chemistry, , vol. 89, # 3 p. 317 - 325