N-(4-甲氧基苯甲酰基)-4-甲基苯磺酰胺合成路线 （共 13 条）
反应条件
potassium iodide in acetonitrile
T=82°C; Friedel-Crafts Acylation; 24 h; Inert atmosphereSealed tube;
参考文献
Wakeham, Russell J.; Taylor, James E.; Bull, Steven D.; Morris, James A.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 3 p. 702 - 705
反应条件
Ru(5,10,15,20-tetrakis(p-tolyl)porphyrinato)(CO) in dichloromethane
T=20°C; 0.5 h;
参考文献
Chang, Joyce Wei Wei; Chan, Philip Wai Hong
Angewandte Chemie - International Edition, 2008 , vol. 47, # 6 p. 1138 - 1140
反应条件
pyridine; copper(l) chloride in acetonitrile
T=20°C; 18 h; Inert atmosphereMolecular sieve;
参考文献
Chang, Joyce Wei Wei; Ton, Thi My Uyen; Tania, Stefani; Taylor, Paul C.; Chan, Philip Wai Hong
Chemical Communications, 2010 , vol. 46, # 6 p. 922 - 924
反应条件
CTMDP; triethylamine in chlorobenzene
T=20 - 130°C; 14 h; Reagent/catalyst; chemoselective reaction;
参考文献
Kosal, Andrew D.; Wilson, Erin E.; Ashfeld, Brandon L.
Chemistry--A European Journal, 2012 , vol. 18, # 45 p. 14444 - 14453,10
Title/Abstract Full Text Show Details
Kosal, Andrew D.; Wilson, Erin E.; Ashfeld, Brandon L.
Chemistry - A European Journal, 2012 , vol. 18, # 45 p. 14444 - 14453
反应条件
aluminium trichloride in dichloromethane
T=20°C; 15 h;
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
potassium carbonate in ethyl acetate
T=80°C; 3 h; Inert atmosphere;
参考文献
Borah, Arun Jyoti; Phukan, Prodeep
Chemical Communications, 2012 , vol. 48, # 44 p. 5491 - 5493
反应条件
ytterbium(III) triflate in dichloromethane
T=20°C; Friedel-Crafts reaction; 2 h;
参考文献
Su; Li; Yang
Journal of the Indian Chemical Society, 2004 , vol. 81, # 10 p. 885 - 887
反应条件
1: CH2Cl2 / 10 h / 20 °C
2: 98 percent / AlCl3 / CH2Cl2 / 15 h / 20 °C
View Scheme
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
1: 10 h / 40 °C
2: 98 percent / AlCl3 / CH2Cl2 / 15 h / 20 °C
View Scheme
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
1: 75 percent / sodium hydrogentelluide (NaTeH) / ethanol; diethyl ether / 0.25 h / Ambient temperature
2: tosylation
View Scheme
参考文献
Suzuki, Hitomi; Takaoka, Koji
Chemistry Letters, 1984 , p. 1733 - 1736
