1,2-二甲氧基-4-乙基苯合成路线 （共 21 条）
反应条件
1: 82 percent / titanium(IV) chloride tris(trifluoromethanesulfonate); trifluoromethanesulfonic acid
2: 98 percent / triethylsilane / trifluoroacetic acid / 12 h / 20 °C
View Scheme
参考文献
Ma, Tingli; Kojima, Takahiko; Matsuda, Yoshihisa
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 3 p. 747 - 748
反应条件
1: NaBH4 / methanol
2: pyridine / benzene / Ambient temperature
3: 7 percent Chromat. / methanol / Irradiation
View Scheme
参考文献
Pincock, J. A.; Wedge, P. J.
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5587 - 5595
反应条件
1: pyridine / benzene / Ambient temperature
2: 7 percent Chromat. / methanol / Irradiation
View Scheme
参考文献
Pincock, J. A.; Wedge, P. J.
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5587 - 5595
反应条件
1: 85 percent / tetrabutylammonium bromide, 40percent aq. NaOH / CH2Cl2 / 2 h / 0 °C
2: 90 percent / Li / liquid ammonia; diethyl ether; ethanol / 2 h / -33 °C
View Scheme
参考文献
Yadav, J. S.; Reddy, P. Satyanarayana; Joshi, Bhalchandra V.
Tetrahedron, 1988 , vol. 44, # 23 p. 7243 - 7254
反应条件
hydrogen; palladium on activated charcoal
参考文献
Kindler,K.; Luehrs,K.
Justus Liebigs Annalen der Chemie, 1967 , vol. 707, p. 26 - 34
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; triphenylphosphine in tetrahydrofuran
20 h; Heating; Title compound not separated from byproducts;
参考文献
Beller, Matthias; Eichberger, Martin; Trauthwein, Harald
Angewandte Chemie (International Edition in English), 1997 , vol. 36, # 20 p. 2225 - 2227
反应条件
in methanol
Irradiation;
参考文献
Pincock, J. A.; Wedge, P. J.
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5587 - 5595
反应条件
1: POCl3 / 170 °C
2: dioxane; aqueous NaOH
3: sodium methylate; methanol
4: aqueous ethanol; palladium/charcoal / 25 °C / Hydrogenolyse
View Scheme
参考文献
Goldberg; Turner
Journal of the Chemical Society, 1946 , p. 111
反应条件
T=25°C; Hydrogenation;
参考文献
Goldberg; Turner
Journal of the Chemical Society, 1946 , p. 111
反应条件
Irradiationdifferent multiple methoxy-substituted benzyl acetates and benzyl pivalates; Product distributionMechanism;
参考文献
Pincock, J. A.; Wedge, P. J.
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5587 - 5595
