反应条件
1: 4-bromo-benzyl bromide With triethyl phosphite T=150°C; 3 h; Inert atmosphere; 2: With sodium hydride in N,N-dimethyl-formamide; mineral oil Horner-Wadsworth-Emmons olefination; 0.333333 h; Cooling with ice; 3: 4-dimethylamino-benzaldehyde in N,N-dimethyl-formamide; mineral oil Horner-Wadsworth-Emmons olefination; 12 h;
参考文献
Gigante, Barbara; Esteves, M. Alexandra; Pires; Davies, Matthew L.; Douglas, Peter; Fonseca, Sofia M.; Burrows, Hugh D.; Castro, Ricardo A. E.; Pina, Joao; Seixas De Melo, Joao
New Journal of Chemistry, 2009 , vol. 33, # 4 p. 877 - 885