4-氯-4'-甲氧基联苯合成路线 (共 62 条)
反应条件
1: 80 percent / NEt3
2: methanol / 1 h / Ambient temperature; Irradiation
View Scheme
参考文献
Shi, Min; Yamamoto, Kiichi; Okamoto, Yoshiki; Takamuku, Setsuo
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 60, # 1.2 p. 1 - 14
反应条件
1: POCl3
2: 80 percent / NEt3
3: methanol / 1 h / Ambient temperature; Irradiation
View Scheme
参考文献
Shi, Min; Yamamoto, Kiichi; Okamoto, Yoshiki; Takamuku, Setsuo
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 60, # 1.2 p. 1 - 14
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); potassium fluoride; tri-tert-butyl phosphine / acetonitrile / 48 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Proutiere, Fabien; Schoenebeck, Franziska
Angewandte Chemie - International Edition, 2011 , vol. 50, # 35 p. 8192 - 8195
参考文献
Spivey, Alan C.; Diaper, Christopher M.; Rudge, Andrew J.
Chemical Communications, 1999 , # 9 p. 835 - 836
反应条件
in methanol
1 h; Ambient temperatureIrradiation; Yield given;
参考文献
Shi, Min; Yamamoto, Kiichi; Okamoto, Yoshiki; Takamuku, Setsuo
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 60, # 1.2 p. 1 - 14
参考文献
Dewar; James
Journal of the Chemical Society, 1958 , p. 917,921
参考文献
Jones; Sleight
Journal of the Chemical Society, 1954 , p. 1775,1780
参考文献
Dewar; James
Journal of the Chemical Society, 1958 , p. 917,921
参考文献
Nakamura, Mitsunobu; Sawasaki, Kouiti; Okamoto, Yoshiki; Takamuku, Setsuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 141 - 146
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lt;(CH3)2COgt;2B-Blt;OC(CH3)2gt;2; potassium acetate; sodium carbonate
multistep reaction: 1.) DMF, 80 deg C, 2 h, 2.) DMF, 80 deg C; reactions of aryl halydes and triflates; Product distribution;
参考文献
Giroux, Andre; Han, Yongxin; Prasit, Petpiboon
Tetrahedron Letters, 1997 , vol. 38, # 22 p. 3841 - 3844