anhyd. cyanate salt reacted with two equiv. amt. of dry org. acid, heated in vac. at 130°C; passed through tube filled with P4O10, collected in liq. N2 trap;
参考文献
Fischer, Gerd; Geith, Janna; Klapoetke, Thomas M.; Krumm, Burkhard
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2002 , vol. 57, # 1 p. 19 - 24
in water
dropwise addn. of satd. soln. of KOCN to conctd. H3PO4, condensing HNCO vapor in a in atrap (-196°C), according to: Ashby, R. A.; Werner,R. L.; J Mol. Spectrosc. 1965, 18, 184; distn. (-30 and -196°C);
参考文献
Sanov; Droz-Georget; Zyrianov; Reisler
Journal of Chemical Physics, 1996 , vol. 106, # 17 p. 7013 - 7022
anhyd. cyanate salt reacted with two equiv. amt. of dry org. acid, heated in vac. at 130°C; collected in liq. N2 trap, distd. in vac.;
参考文献
Fischer, Gerd; Geith, Janna; Klapoetke, Thomas M.; Krumm, Burkhard
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2002 , vol. 57, # 1 p. 19 - 24
Gmelin Handbook: C: MVol.D1, 34.2.2, page 328 - 329
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Normand, C. W. B.; Cumming, A. C.
Journal of the Chemical Society, 1912 , vol. 101, p. 1852 - 1866
