4,4-二甲基-2-戊酮合成路线 （共 111 条）
参考文献
Howard et al.
Journal of Research of the National Bureau of Standards (United States), 1947 , vol. 38, p. 391
Chem. Zentralbl., 1947 , vol. 118, p. 5291
参考文献
Duismann,W. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1820 - 1833
反应条件
1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.58 h / 0 °C / |Inert atmosphere
1.2: |Inert atmosphere; |Reflux
2.1: 10 Pd/C; hydrogen / methanol / 1500.15 Torr / |Inert atmosphere
View Scheme
参考文献
Li, Jia-Qi; Quan, Xu; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 34 p. 10609 - 10616
参考文献
Huston et al.
Journal of Organic Chemistry, 1941 , vol. 6, p. 252
Journal of the American Chemical Society, 1948 , vol. 70, p. 1090
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 2039
反应条件
1: sodium borate; diethyl ether
3: potassium acetate; acetic acid anhydride; acetic acid
View Scheme
参考文献
Whitmore; Homeyer
Journal of the American Chemical Society, 1933 , vol. 55, p. 4195,4558
反应条件
1: NaOBr
2: SOCl2
3: water; NH3 / <10
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参考文献
Homeyer; Whitmore; Wallingford
Journal of the American Chemical Society, 1933 , vol. 55, p. 4209,4212
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
T=49.7°C; Baeyer-Villiger oxidation; P=750.06 Torr; KineticsThermodynamic data; Further Variations:PressuresTemperatures;
参考文献
Jenner, Gerard
Tetrahedron Letters, 2001 , vol. 42, # 51 p. 8969 - 8971
反应条件
1: 59 percent / LDA
2: 81 percent / TiCl4 / 3 h / -40 °C
View Scheme
参考文献
Liberman,A.L.; Vasina,T.V.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, # 10 p. 3233 - 3237,3179 - 3182
反应条件
1,4-dioxane; diethyl ether; bromine
参考文献
Asinger,F.; Gentz,F.
Monatshefte fuer Chemie, 1965 , vol. 96, p. 1461 - 1473
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Sarel; Newman
Journal of the American Chemical Society, 1956 , vol. 78, p. 5416,5418
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Overberger; Berenbaum
Journal of the American Chemical Society, 1952 , vol. 74, p. 3293
