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乙二醇
甲醛
63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
碘苯
合成路线
（共 4240 条）
591-50-4
碘苯
+
99-93-4
对羟基苯乙酮
→
反应条件
5031-78-7
4'-苯氧基苯乙酮
反应条件
potassium phosphate; copper(l) iodide; 2-((2-isopropylphenylimino)methyl)phenol in 1,4-dioxane T=20 - 101°C; Ullmann Condensation; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Qian, Cun-Wei; Lv, Wen-Lin; Zong, Qian-Shou; Wang, Mao-Yuan; Fang, Dong
Chinese Chemical Letters, 2014 , vol. 25, # 2 p. 337 - 340
591-50-4
碘苯
+
13329-40-3
4-碘代苯乙酮
→
反应条件
5031-78-7
4'-苯氧基苯乙酮
反应条件
copper(l) iodide; CsOH; 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate in dimethyl sulfoxide T=130°C; 30 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Tlili, Anis; Monnier, Florian; Taillefer, Marc
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12299 - 12302
591-50-4
碘苯
+
95-13-6
茚
→
反应条件
4505-48-0
反应条件
sodium carbonate; palladium diacetate; 2-phenyl-4S-isobutyloxazoline in various solvent(s) T=120°C; 115 h;
参考文献
Montell Technology Company bv
Patent: US6271411 B1, 2001 ;
591-50-4
碘苯
+
95-13-6
茚
→
反应条件
1961-97-3
+
4505-48-0
反应条件
triethylamine; palladium diacetate in N,N-dimethyl-formamide T=100°C; 4 h;
参考文献
Nifant'ev, Ilya E; Sitnikov, Alexander A; Andriukhova, Nonna V; Laishevtsev, Ilya P; Luzikov, Yuri N
Tetrahedron Letters, 2002 , vol. 43, # 17 p. 3213 - 3215
591-50-4
碘苯
+
201230-82-2
+
5467-74-3
→
反应条件
90-90-4
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in various solvent(s) T=80°C; P=760 Torr; 5 h;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
591-50-4
碘苯
+
589-87-7
→
反应条件
90-90-4
反应条件
1: iodobenzene With gallium; aluminium T=120°C; 20 h; Inert atmosphere; 2: 4-bromo-1-iodobenzene in toluene T=20°C; 3 h;
参考文献
Tang, Xiaoping; Rawson, Daniel; Woodward, Simon
Synlett, 2010 , # 4 art. no. D32709ST, p. 636 - 638
622-97-9
+
591-50-4
碘苯
→
反应条件
4714-21-0
反应条件
palladium diacetate; potassium carbonate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in N,N-dimethyl-formamide T=80°C; Heck Reaction; Sealed tube;
参考文献
Amini, Mojtaba; Bagherzadeh, Mojtaba; Rostamnia, Sadegh
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 433 - 436
591-50-4
碘苯
+
766-97-2
→
反应条件
4714-21-0
反应条件
1: 4-methyl phenyl acetylene With Schwartz's reagent; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=30°C; 1 h; Inert atmosphere; 2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) T=60°C; 12 h; Inert atmosphere;
参考文献
Huang, Bin; Wang, Pingping; Hao, Wenyan; Cai, Ming-Zhong
Journal of Organometallic Chemistry, 2011 , vol. 696, # 13 p. 2685 - 2688
622-97-9
+
591-50-4
碘苯
+
501-65-5
→
反应条件
4714-21-0
+
78906-75-9
反应条件
sodium hydrogencarbonate; triphenylphosphine; lithium chloride; palladium diacetate in water; N,N-dimethyl-formamide T=130°C; 5 h;
参考文献
Shibata, Kana; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2005 , vol. 7, # 9 p. 1781 - 1783
591-50-4
碘苯
+
1032938-01-4
→
反应条件
4714-21-0
反应条件
sodium hydroxide; tetrabutyl ammonium fluoride; dihydrogen peroxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=55°C; Hiyama coupling; 10 h;
参考文献
Wang, Zhizhong; Pitteloud, Jean-Philippe; Montes, Lucresia; Rapp, Magdalena; Derane, Djenny; Wnuk, Stanislaw F.
Tetrahedron, 2008 , vol. 64, # 22 p. 5322 - 5327
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