(6CI,7CI)-2-对甲苯萘合成路线 （共 62 条）
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran; diethyl ether
48 h; Heating;
参考文献
Cho, Chul-Hee; Park, Heon; Park, Min-Ah; Ryoo, Tae-Yong; Lee, Yoon-Sik; Park, Kwangyong
European Journal of Organic Chemistry, 2005 , # 15 p. 3177 - 3181
反应条件
1: RLi or RMgBr, R = 4-MeC6H4 With indium(III) chloride in tetrahydrofuran
T=-78°C; 0.5 h; Inert atmosphere;
2: naphthalene-2-yl methanesulfonate With Ni(PCy3)2Cl2; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=20 - 80°C; Inert atmosphere;
参考文献
Zhang, Liang; Luo, Yong; Wu, Jie
Synlett, 2010 , # 12 p. 1845 - 1848
反应条件
potassium phosphate; Ni(PCy3)2Cl2; PCy3∙HBF4 in o-xylene
T=150°C; Suzuki-Miyaura cross-coupling; 20 h; Inert atmosphere;
参考文献
Quasdorf, Kyle W.; Antoft-Finch, Aurora; Liu, Peng; Silberstein, Amanda L.; Komaromi, Anna; Blackburn, Tom; Ramgren, Stephen D.; Houk; Snieckus, Victor; Garg, Neil K.
Journal of the American Chemical Society, 2011 , vol. 133, # 16 p. 6352 - 6363
反应条件
in tetrahydrofuran
T=110°C; 24 h; Inert atmosphere;
参考文献
Minami, Hiroki; Wang, Xuan; Wang, Chao; Uchiyama, Masanobu
European Journal of Organic Chemistry, 2013 , # 35 p. 7891 - 7894
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran
T=35°C; 24 h; Inert atmosphere;
参考文献
Ding, Han; Chen, Yali; Cao, Weiguo; Wu, Kaicheng; Chen, Jie; Lee, Albert W. M.
Synthetic Communications, 2010 , vol. 40, # 7 p. 984 - 991
反应条件
hydrogen; palladium on activated charcoal
T=250°C; P=3750.3 Torr;
参考文献
Chebaane,K. et al.
Bulletin de la Societe Chimique de France, 1975 , p. 2521 - 2526
反应条件
1: NaH / tetrahydrofuran / 12 h / 26 °C
2: Bu4NF / tetrahydrofuran / 10 h / 27 °C
3: 35 percent / TpRu(PPh3)(CH3CN)2PF6 / toluene / 6 h / 110 °C
View Scheme
参考文献
Shen, Hung-Chin; Pal, Sitaram; Lian, Jian-Jou; Liu, Rai-Shung
Journal of the American Chemical Society, 2003 , vol. 125, # 51 p. 15762 - 15763
反应条件
1: NaH / tetrahydrofuran / 12 h / 26 °C
2: Bu4NF / tetrahydrofuran / 10 h / 27 °C
3: 35 percent / TpRu(PPh3)(CH3CN)2PF6 / toluene / 6 h / 110 °C
View Scheme
参考文献
Shen, Hung-Chin; Pal, Sitaram; Lian, Jian-Jou; Liu, Rai-Shung
Journal of the American Chemical Society, 2003 , vol. 125, # 51 p. 15762 - 15763
反应条件
1: 91 percent / pyridine / CHCl3 / 12 h / 20 °C
2: 81 percent / dppfNiCl2 / tetrahydrofuran; diethyl ether / 24 h / Heating
View Scheme
参考文献
Cho, Chul-Hee; Yun, Hee-Sung; Park, Kwangyong
Journal of Organic Chemistry, 2003 , vol. 68, # 8 p. 3017 - 3025
反应条件
palladium diacetate; silver trifluoroacetate in 2,2,2-trifluoroethanol
T=120°C; 14 h;
参考文献
Qin, Chunxia; Lu, Wenjun
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7424 - 7427
