in neat (no solvent)
heating to 200°C in an autoclave;;
参考文献
Ashby, E. C.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4791 - 4795
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Gmelin Handbook: B: B-Verb.14, 3.8.1.2.3, page 100 - 104
lt;RhH(PEt3)3gt;; hydrogen in ethanol
T=125°C; P=30400 Torr; 3 h; Title compound not separated from byproducts;
参考文献
MacDougall, Joanna K.; Simpson, Michael C.; Green, Michael J.; Cole-Hamilton, David J.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 6 p. 1161 - 1172
aluminium phenoxide
T=200°C; 8 h; different temperatures; other times; various molar ratios of reagents; also for 2-octene; Product distributionMechanism;
参考文献
Kozlikovskii, Ya. B.; Koshchii, V. A.; Ovsiyuk, T. F.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 1.1 p. 49 - 54
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 1 p. 55 - 61
lt;RhH(PEt3)3gt;; hydrogen in ethanol
T=125°C; P=30400 Torr; 3 h; Title compound not separated from byproducts;
参考文献
MacDougall, Joanna K.; Simpson, Michael C.; Green, Michael J.; Cole-Hamilton, David J.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 6 p. 1161 - 1172