反应条件
1: 1.) butyllithium / 1.) THF, hexane, -70 deg C, 15 min, 2.) a) -70 deg C, 5 h, b) from -70 deg to RT, 1.5 h, c) RT, 15 h 2: 90 percent / H2 / 2percent Pd-C / hexane / 120 h / Ambient temperature 3: 69 percent / lithium aluminum hydride / diethyl ether / 1.) reflux, 5 h, 2.) from 20 deg C to 25 deg C, 15 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 7.1 p. 1209 - 1210
Zhurnal Organicheskoi Khimii, , vol. 26, # 7 p. 1402 - 1404
