1: N'-cyclohexylidene-N,N-diethyl-1,2-ethanediamine With 2,4,6-trimethylphenylmagnesium bromide in tetrahydrofuran T=80°C; 1 h; 2: 1-decylfluoride in tetrahydrofuran T=65°C; 36 h; 3: With acetic acid in tetrahydrofuran T=50°C; 1 h;

2: 1.) n-BuLi, 3.) KH2OP4, H3PO3 / 1.) THF, -30 deg C, 1 h, 2.) 25 deg C, 2 h, 3.) 25 deg C, overnight View Scheme

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potassium dihydrogenphosphate; n-butyllithium; orthophosphorus acid 1.) THF, -30 deg C, 1 h, 2.) 25 deg C, 2 h, 3.) 25 deg C, overnight; Yield given. Multistep reaction;