反应条件
tert.-butyl lithium in diethyl ether; hexane; pentane (N2), stannane in hexane cooled to 0°C, soln. of t-BuLi in pentane added, Et2O added dropwise, warmed to room temp., 24 h; hydrolyzed with satd. NH4Cl soln., diluted with hexane, org. layer sepd., washed with water for 3 times, dried, concd. under reduced pressure, collected from GLPC, elem. anal.;
参考文献
Farah, Dan; Karol, Thomas J.; Kuivila, Henry G.
Organometallics, 1985 , vol. 4, p. 662 - 666
