Gilman, H.; Moore, F. W.; Jones, R. G.
Journal of the American Chemical Society, 1941 , vol. 63, p. 2482 - 2485
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.16.1.4.5, page 159 - 161
anal.R.mit Tetrakis-<4-chlor-phenyl>-zinn, Tetraphenylblei, Diphenyl-di-p-tolyl-blei, Tetra-p-tolyl-blei, Triphenylblei und Tri-p-tolyl-blei;
参考文献
Gilman; Moore; Jones
Journal of the American Chemical Society, 1941 , vol. 63, p. 2482,2484
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Gilman; Moore
Journal of the American Chemical Society, 1940 , vol. 62, p. 3206
in benzene BCl3 cooled at -78°C and quickly added to Sn(C6H5)4, cooled at 5°C while stirring; warming at ambient temp., boiled for 3.5 h using back-flow; best lab. method; solvent must be distd. below 140°C (immersion thermometer!); crude product distd. between 150-200°C; fractional vac. distn.;
Burch, J. E.; Gerrard, W.; Howarth, M.; Mooney, E. F.
Journal of the Chemical Society, 1960 , p. 4916 - 4918
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.16.1.4.4, page 157 - 159
