3,3-二甲基-1,2-丁二醇合成路线 （共 13 条）
反应条件
potassium osmate(VI); diethyl-(2-benzyloxy-ethyl)-amine; 4-methylmorpholine N-oxide in acetone T=20°C; 72 h;
参考文献
Stiasny, Hans Christian
Synthesis, 1996 , # 2 p. 259 - 264
反应条件
potassium hydroxide in dimethyl sulfoxide T=100°C;
参考文献
Mischitz; Kroutil; Wandel; Faber
Tetrahedron Asymmetry, 1995 , vol. 6, # 6 p. 1261 - 1272
反应条件
ethanol; nickel T=100°C; Hydrogenation.unter Druck;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 3121
反应条件
dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; water T=25°C; 2 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 14, # 34 p. 10648 - 10655
反应条件
in n-heptane; dichloromethane 16 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 53, # 22 p. 7429 - 7444
反应条件
1: potassium hydroxide; polyethylene glycol / 120 - 190 °C 2: aqueous hydrogen peroxide; formic acid / und Erwaermen des Reaktionsprodukts mit wss.Natronlauge View Scheme
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 13, p. 608
反应条件
n-butyllithium 1) pentane, -20 degC -> room temp., 6 h, 2) -80 degC -> room temp.; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 113, # 4 p. 1290 - 1303
反应条件
[Py(NP(iPr)2)(NHP(iPr)2)Ir(cod)]; potassium tert-butylate in tetrahydrofuran T=90°C; 24 h; Inert atmosphere;
参考文献
Hille, Toni; Irrgang, Torsten; Kempe, Rhett
Chemistry - A European Journal, 2014 , vol. 20, # 19 p. 5569 - 5572
反应条件
sodium periodate; sulfuric acid
参考文献
Braendstroem
Acta Chemica Scandinavica (1947-1973), 1959 , vol. 13, p. 608
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; cobalt(II) 2,4-pentanedionate in acetonitrile Oxidation; P=760.051 Torr; 13 h; Heating;
参考文献
Iwahama, Takahiro; Yoshino, Yasushi; Keitoku, Takashi; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6502 - 6507
